HPLC Column for Pesticide Residue Analysis "Wakopak® Wakosil® Agri-9"
Example of Simultaneous Analysis of 12 Pesticide Analytical Standards
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Column :Wakopak® Wakosil® Agri-9 (4.6 mm x 250 mm) Eluent :Wakosil® Agri-9 Eluent for 4.6 mm x 250 mm Flow Rate :1.0 mL/min. at 35 ℃ Detection :UV 230 nm - 270 nm MAX Photodiode Array Sample :1) Asulam
4) MCPP
7) Propyzamide
10) Pencycuron2) Oxine-Cu
5) Thiuram
8) Iprodione
11) Bensulide3) CAT
6) Siduron
9) TPN
12) Butamifos
Example of Analysis of 28 Pesticides Mixture Standard Solution WQ-3 (each 20μg/mL Acetonitrile Solution)
![01094_img02.png](images/01094_img02.png)
1) Methomyl 2) MPP oxon sulfoxide 3) Tricyclazole 4) MPP oxon sulfone 5) Carbofuran 6) Thiuram 7) Probenazole 8) Thiodicarb 9) MPP sulfoxide 10) MPP oxon 11) Bensulfuron methyl 12) Flazasulfuron 13) Siduron 14) MPP sulfone |
15) Azoxystrobin 16) Dymron 17) Fenthion (MPP) 18) Carpropamide 19) Asulam 20) Bentazone 21) 2,4-Dichlorophenoxyacetic acid (2,4-PA) 22) Triclopyr 23) Mecoprop (MCPP) 24) Diuron (DCMU) 25) Halosulfuron methyl 26) Iprodione 27) Bensulide 28) Fipronil |
"Carbaryl (NAC)" is not included in this product because it is unstable in acetonitrile.
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HPLC
Column: Wakopak® Wakosil® Agri-9 (2.0 mm x 150 mm) Eluent: A) 10 mM CH3COONH4 (pH3.7)
B) CH3CNGradient: Time B conc. 0 - 5 min.
5 - 25 min.
25 - 40 min.
40 - 45 min.
45 - 55 min.12 %
12 - 30 %
30 - 70 %
100 %
12 %Flow Rate: 0.2 mL/min. at 40 ℃ Injection Volume: 1 µg/mL, 2 µL -
MS/MS
ESI, MRMIonSpray Voltage 5500 V (pos) -4500 V (neg) Temperature 700 ℃ 300 ℃ Curtein Gas (psig) 40 20 CollisonGas (psig) 5 3 Ion Source Gas 1 (psig) 80 40 Ion Source Gas 2 (psig) 70 80 System 3200 QTRAP® (AB SCIEX)
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HPLC Column
Eluent
Pesticides Mixture Standard Solution
Solid-Phase Extraction Column for Pretreatment
For research use or further manufacturing use only. Not for use in diagnostic procedures.
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