Special Reagent for Hitachi High-Tech Science HM1000A

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Thermal Desorption MS HM1000A

The "Thermal Desorption MS HM1000A" that is manufactured by Hitachi High-Tech Science Corporation is a device dedicated to the rapid screening test of phthalate esters, which are regulated by the RoHS 2 Directive.
We sell a mixture sample for obtaining the calibration curve for HM1000A, along with reagent for the calibration.

Product Description

Mixture of 8 types of Phthalate Esters

PVC resin contains 8 types of phthalic acids (DEHP, BBP, DBP, DIBP, DNOP, DINP, DIDP, DnHP each 1,000 pppm) and is employed for obtaining the calibration curve.

Sample for Calibration

Of the 4 types of phthalate esters (DEHP, DBP, BBP, DIBP) that are regulated by the RoHS 2 Directive, DEHP contains DOTP and DnOTP as an impurity. DOTP and DnOTP are not controlled substances. Therefore, it is necessary to correct the amount of DOTP and DnOTP at the time of measurement.
DOTP and DnOTP produce fragment ions. Corrected measurement results are obtained by using the sample for calibration and subtracting the amount of DOTP and DnOTP from the assay results of DEHP.

Method of Use

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  1. Cut the sample.
  2. Set the cut sample in the center of the sample pan and weigh it.*
    *Adjust the weight of the sample to 0.16-0.24 mg (excluding the weight of the sample pan).
  3. Place it in the sample tray of the equipment.

Physical Properties of DOTP and DnOTP

Name DEHP DOTP DnOTP
Bis(2-ethylhexyl) Phthalate
(RoHS 2 restricted substances)
Bis(2-ethylhexyl) Terephthalate
(Non-restricted substances)
Di-n-octyl Phthalate
(Non-restricted substances)
Structural
formula
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Molecular
weight
390.56 390.56 390.56
Molecular
formula
C24H38O4 C24H38O4 C24H38O4
Boiling
point
386 ℃
(Literature deta)
400 ℃
(Literature deta)
437 ℃
(Literature deta)

  • Owing to the convenience of the manufacturing method of this sample, part of this sample may be discolored. Remove the discolored part before use.
  • This product is also available for HM1000.

HM1000A

For details of HM1000, please refer to the website of Hitachi High-Tech Science Corporation.

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for Obtaining a Calibration Curve

Sample for Calibration

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Standard substance for Green Procurement

For research use or further manufacturing use only. Not for use in diagnostic procedures.

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