Analytical Standards for Phthalates Testing
Phthalates (Phthalate esters) is a general term for esters of an o-phthalic acid and an alcohol. Phthalates is widely used as a plasticizer for polyvinyl chloride, but due to its harmfulness to the human body, various regulations such as the Japanese Food Sanitation Act and the RoHS have been imposed all over the world. FUJIFILM Wako provides analytical standards for phthalates analysis.
8 Phthalates Mixture Standard Solution
GC/MS Chromatogram
| Peak No. | Phthalate Ester | Abbreviation | Peak No. | Phthalate Ester | Abbreviation |
|---|---|---|---|---|---|
| 1 | Diethyl Phthalate | DEP | 5 | Di-n-hexyl Phthalate | DNHP |
| 2 | Dipropyl Phthalate | DPrP | 6 | Benzyl Butyl Phthalate | BBP |
| 3 | Di-n-butyl Phthalate | DBP | 7 | Bis(2-ethylhexyl) Phthalate | DOP, DEHP |
| 4 | Di-n-pentyl Phthalate | DEP | 8 | Dicyclohexyl Phthalate | DCHP |
Analysis conditions
[GC]
- Column
- ： BPX-5 0.25 μm, 0.32 mm × 30 m
- Column temperature
- ： 100℃ (2 min.)→10℃/min.→270℃ (11 min.)
- Injection temperature
- ： 210℃
- Carrier gas
- ： He 2.0 mL/min.
- Splitless
- ： 0.5 min.
[MS]
- Ionization
- ： EI
- Interface temperature
- ： 250℃
Abbreviation for Major Phthalates
GC Chart for Major Phthalates
Compendial Regulations (As of June 2022)
Japanese Food Sanitation Law (Toys)
Standard values for harmful substances contained in toys are set so that infants do not adversely affect their health when they touch the toys.
JP Water Quality (Complementary Items)
In order to guarantee the quality of tap water, the target value of harmful substances contained in tap water is set.
RoHSⅡ (Restriction of the use of certain hazardous substances in electrical and electronic equipment)
Regulations on specific harmful substances contained in electrical/electronic device in Europe. Standard values for 10 types of harmful substances contained in electrical/electronic device are set.
CPSIA (Consumer Product Safety Improvement Act)
The Consumer Product Safety Improvement Act in the United States. Standard values for harmful substances contained in toys are set.
| Phthalate Ester | JP | EU | US | |
|---|---|---|---|---|
| Food Sanitation Law (Toys) |
Water Quality (Complementary Items) |
RoHSⅡ | CPSIA (Section 108) |
|
| Di-n-butyl Phthalate (DBP） | ✔ | ✔ | ✔ | |
| Diisobutyl Phthalate (DIBP） | ✔ | ✔ | ||
| Benzyl Butyl Phthalate (BBP) | ✔ | ✔ | ✔ | |
| Di-n-pentyl Phthalate (DPP） | ✔ | |||
| Di-n-hexyl Phthalate (DHP） | ✔ | |||
| Bis(2-ethylhexyl) Phthalate (DOP, DEHP) | ✔ | ✔ | ✔ | ✔ |
| Dicyclohexyl Phthalate (DCHP) | ✔ | |||
| Di-n-octyl Phthalate (DNOP) | ✔ | |||
| Diisononyl Phthalate (DINP) | ✔ | ✔ | ||
| Diisodecyl Phthalate (DIDP) | ✔ | |||
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Mixture Standard Solution
Standards for phthalate
For research use or further manufacturing use only. Not for use in diagnostic procedures.
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If the revision of product standards and packaging standards has been made, there is a case where the actual product specifications and images are different.
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